A highly clean and efficient and eco-friendly method for the synthesis of 1-Tosyl-2-Ethyl-pyrolidine which is an alkaloid is taken for investigation. The synthesis of this compound is done by using THF and LAH. Numbers of experimental methods are used for alignment and centring of said compound. Six cell parameters, three axial lengths a, b, c and three interaxial angles α, β, and ϒ are determined to see that compound taken under investigation belong to which crystal system. To investigate X-ray diffraction technique is used. The purpose of working on the compound is that it has pharmacological as well as botanical importance. Weissenberg camera is used for the purpose.